By Douglas C. Neckers, William S. Jenks, Thomas Wolff

ISBN-10: 047139467X

ISBN-13: 9780471394679

Content material: Photochemistry of triarylmethane dye leuconitriles / Viktor V. Jarikov and Douglas C. Neckers -- constitution and reactivity of natural intermediates as printed by means of time-resolved infrared spectroscopy / John P. Toscano -- Semiconductor photocatalysis for natural synthesis / Horst Kisch -- Photophysical probes of DNA sequence-directed constitution and dynamics / Catherine J. Murphy

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Moreover, 10a-d (Fig. 3) could be purified by silica gel chromatography, and were applied to the synthesis of deoxyribonucleotides on silica (7), controlled-pore glass (CPG) (8), or cellulose filter disks (9). Similarly, Sa-d (Fig. 3) did not show significant decomposition in acetonitrile after 4 d (6). Under these conditions, Sb (Fig. 3) was more stable than 6b (Fig. 3), which in turn was more stable than 3b (6). The efficacy of the deoxyribonucleoside phosphoramidites Sa-d (Fig. 3) was demonstrated by the synthesis of 5 1 mers on CPG, which, at the time, were the largest DNA segments ever chemically synthesized (6).

3. Gait, M J , Matthes, H. , and Tltmas, R. C (1982) Nucleic Acids Res. 10,6243-6254 4 Gait, M. J. ) (1984) Oligonucleotide Synthesis A Practical Approach IRL Press, Oxford Chapter 4 5 For a review, see Caruthers, M. H (1991) Act Chem Res. , Brunden, M. J , and Gllham, P T. (1981) Tetrahedron Left. 22, 4177-4180 7. , and Wolter, A. (1983) Tetrahedron Lett 24,747-750. 8. Sproat, B. S and Bannwarth, W. (1983) Tetrahedron Lett. 24,5771-5774. , Sheppard, R. , and Rosevear, A. (1981) J Chem. Sot Commun, 1151-l 152 10.

1984) Solution synthesis of protected di-2’deoxynucleoside phosphotriesters via the phosphoramidite approach. Tetrahedron Lett 25, 1975-1978. 26. Schwarz, M. W. and Pfleiderer, W. (1984) Solution synthesis of fully protected thymidine dimer usmg various phosphoramidites. Tetrahedron Lett. 25, 5513-5516. 27. , Marugg, J. E , van Boom, J. , Honnens, J , Taagaard, M , and Dahl, 0 (1986) Thermal instability of some alkyl phosphorodiamidites. J. Chem. Res. (S), 26,27. 28. Hamamoto, S. and Takaku, H (1986) New approach to the synthesis of deoxyribonucleoside phosphoramidite derivatives.

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